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Beilstein J. Org. Chem. 2016, 12, 2150–2163, doi:10.3762/bjoc.12.205
Graphical Abstract
Scheme 1: Grignard metathesis polymerization method of synthesizing the diblock copolymer. Relative block len...
Figure 1: Differential scanning calorimetry thermogram (second cycle, 10 K/min) of P3OT-b-F-P3OT 2:1 before (...
Figure 2: Selected region of the 1H NMR (d2-TCE at 403 K) of P3OT-b-F-P3OT produced with 3:1 (a) and 1:3 (b) ...
Figure 3: Thin film UV–visible absorption spectra of 2:1 (a) and 1:4 (b) P3OT-b-F-P3OT polymers (red line), o...
Figure 4: Overlay of thin film UV–visible absorption spectra (a) of the two block copolymers and the correspo...
Figure 5: Thin-film UV–visible absorption spectra of a) P3OT, b) F-P3OT, c) P3OT-b-F-P3OT 2:1, d) P3OT-b-F-P3...
Figure 6: Temperature dependent Raman spectra measured during heating showing the main C–C and C=C stretches ...
Figure 7: Influence of temperature on the relative Raman scattering intensities of the P3OT (1446 cm−1) and F...